May 25, 2021 · The injection volume in split mode (split ratio 1:10) was 0.5 µl with the injector temperature at 250 °C, and the gaz carrier was He at 36.5 cm/s. interface temperature, 280 °C; ion source temperature, 250 °C; mass range, m/z 50–600; scan speed, 2500 amu/seg; and event time, 0.20 seg., were the MS detection parameters employed for the ...
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